HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58522072, compound → HCID 46866481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58522072 | HCID 58522072 | — |
| Solvent | Diethylether pentane | HCID 21877078 | — |
| Product | HCID 46866481 | HCID 46866481 | 77% |
Reaction Steps
Following the general method as outlined in Example 15, starting from tert-butyl{4-chloro-2-[(5-{[isobutyl(methyl)amino]sulfonyl}-2-methylphenyl)ethynyl]phenoxy}acetate (Intermediate 160), the title compound was obtained as a beige solid in 77% yield after tituration in pentane/diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-38afbaf8df53497081f8a314255576b6 |
| Source note | uspto-grants-2012_09 |