HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58522068, compound → HCID 46866482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58522068 | HCID 58522068 | — |
| Solvent | Diethylether pentane | HCID 21877078 | — |
| Product | HCID 46866482 | HCID 46866482 | 96% |
Reaction Steps
Following the general method as outlined in Example 15, starting from tert-butyl{2-[(5-{[butyl(methyl)amino]sulfonyl}-2-methylphenyl)ethynyl]-4-chlorophenoxy}acetate (Intermediate 161), the title compound was obtained as a beige solid in 96% yield after trituration in diethyl ether/pentane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a05e6c64d6ce46c2aaef1ccd872664a5 |
| Source note | uspto-grants-2012_09 |