HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-3-(propylsulfonyl)benzene → HCID 46865086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-3-(propylsulfonyl)benzene | HCID 56594267 | — |
| Reactant | HCID 58522099 | HCID 58522099 | — |
| Product | HCID 46865086 | HCID 46865086 | — |
Reaction Steps
Following the general method as outlined in Example 37, starting from tert-butyl[(3-bromobiphenyl-4-yl)oxy]acetate (Intermediate 188) and 1-ethynyl-3-(propane-1-sulfonyl)-benzene (Intermediate 42), the title compound was obtained as a beige solid after purification by preparative HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273769B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-f3fd2a43d7ad42859d998eb6c5b7bff9 |
| Source note | uspto-grants-2012_09 |