HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 66910028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Butyric acid, 4-(p-isopropylbenzoyl)- | HCID 177018 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66910028 | HCID 66910028 | — |
Reaction Steps
5-(4-Isopropyl-phenyl)-5-oxo-pentanoic acid (5 g, 21.3 mmol) was dissolved in 75 mL ethanol in a 250 mL flask. Sodium hydroxide (0.85 g, 21.3 mmol) was added and the reaction was stirred overnight under reduced pressure on a rotary evaporator. The solid was dried under vacuum and used without further purification. Found: C, 60.24; H, 6.66; Na, 9.21%; C14H17O3Na requires C, 61.28; H, 6.98; Na, 8.38%;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273794B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-a73929ad3f1c4662979d3b0acaf63ca6 |
| Source note | uspto-grants-2012_09 |