HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinecarboxaldehyde → HCID 86103414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86103414 | HCID 86103414 | 100% |
Reaction Steps
300 g pyridine-4-carbaldehyde and 372 g 2,2-diethoxy-ethylamine were refluxed in 2 L toluol over night. The mixture was evaporated to give 621 g of the desired product. The residue was purified by chromatographie on silica to give 100 g desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642774B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-c7779dd223284c77b3a8b0e4e8c418c3 |
| Source note | uspto-grants-2014_02 |