Hydrogen Bromide → HCID 86686499, compound

Participants

Reaction Steps

13.7 g tert-butyl 3-methyl-5-oxoazepane-1-carboxylat was dissolved in 350 mL acetic acid and 99 mL hydro bromide solution (33%) in acetic acid was added. The mixture was stirred for 1.5 h at RT. The volatiles were removed in vacuo and the residue was used in the next step without further purification. (M+H)+: 128

Provenance & Evidence