Bromine → HCID 86686500, compound

Participants

Reaction Steps

6-methylazepan-4-one hydrobromic acid was dissolved in 100 mL acetic acid. A solution of 3.2 mL bromine in 10 mL acetic acid was added. The mixture was stirred for 1.5 h at RT. The volatiles were removed in vacuo and the residue was crystallized with acetonitrile to yield 18.5 g of the desired product. (M+H)+: 228

Provenance & Evidence