HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 239148Generated: October 28, 2026
2-Chloropyrimidine → HCID 71634900, compound
https://huagongshe.com/reaction/239148
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Chloropyrimidine | HCID 74404 | — |
| Reactant | tert-Butyl 2-methylpiperazine-1-carboxylate | HCID 15087784 | — |
| Product | HCID 71634900 | HCID 71634900 | 98.8% |
Reaction Steps
100 mg 2-chloro-pyrimidine was added to 175 mg 2-Methyl-piperazine-1-carboxylic acid tert-butyl ester and this mixture was stirred for 2 h at 120° C. to give 240 mg of the desired compound. Rt: 1.31 min (method B), (M+H)+: 279
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08642774B2 |
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| Source dataset | uspto-grants-2014_02 |
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| ORD ID | ord-bad9a4969d944e078a02c282acb79610 |
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| Source note | uspto-grants-2014_02 |
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