HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 86686061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 86686064 | HCID 86686064 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86686061 | HCID 86686061 | — |
Reaction Steps
9.8 mL bromine was added to 30 g 7-methyl-azepan-4-one hydrobromide in 180 mL acetic acid. The reaction was stirred over night at RT. The reaction was evaporated to yield 33 g of the desired product as isomere mixture. Rf: 0.4 (DCM/MeOH=20/1), (M+H)+=206
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642774B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-7fb9c0926f9a4b4a9d7760eb71a17001 |
| Source note | uspto-grants-2014_02 |