HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 68766282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Fluoro-2-(trifluoromethyl)benzyl bromide | HCID 2737576 | — |
| Reactant | methyl 3-hydroxy-5-(3H-imidazo[4,5-c]pyridin-3-yl)thiophene-2-carboxylate | HCID 68765327 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68766282 | HCID 68766282 | — |
Reaction Steps
In a similar manner as described for example B11, 110.5 mg of 4-fluoro-2-(trifluoromethyl)benzyl bromide, 100 mg of methyl 3-hydroxy-5-(3H-imidazo[4,5-c]pyridin-3-yl)thiophene-2-carboxylate, 59.7 mg of potassium carbonate in 3 ml anhydrous DMF yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273890B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-61dd36b9e5834cf4ac90397d6f4fbd87 |
| Source note | uspto-grants-2012_09 |