HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-chloro-3-oxo-2,3-dihydrothiophene-2-carboxylate → HCID 68766230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-chloro-3-oxo-2,3-dihydrothiophene-2-carboxylate | HCID 15588102 | — |
| Reactant | HCID 178495987 | HCID 178495987 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 68766230 | HCID 68766230 | — |
Reaction Steps
In a similar manner as described for example C3, 1.81 g of 1H-imidazo[4,5-c]pyridine-6-carboxylic acid (2-methoxy-ethyl)-amide and 1.27 g of methyl 2-chloro-3-oxo-2,3-dihydrothiophene-2-carboxylate in 300 ml chloroform yield the title compound which was used for the next step without further purification (example B8).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08273890B2 |
| Source dataset | uspto-grants-2012_09 |
| ORD ID | ord-04e0f452b8a6484aad4092f59c98cd29 |
| Source note | uspto-grants-2012_09 |