HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenolate Sodium → HCID 86654805, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenolate Sodium | HCID 4445035 | — |
| Reactant | HCID 86654806 | HCID 86654806 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86654805 | HCID 86654805 | — |
Reaction Steps
To a solution of tetrabutylammonium-4-chlorobutylsulfonate in THF a solution of sodium phenolate in THF is added dropwise under cooling. After complete addition, the solution is allowed to warm to room temperature. The precipitate is filtered off and the remaining solution is concentrated with a rotary evaporator to yield tetrabutylammonium-4-phenoxybutylsulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642778B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-28b188bfb5b5459b9bc31049714053a8 |
| Source note | uspto-grants-2014_02 |