HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 56973005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 86654806 | HCID 86654806 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 56973005 | HCID 56973005 | — |
Reaction Steps
To a solution of tetrabutylammonium-4-chlorobutylsulfonate in THF sodium carbonate is added. To the resulting suspension, a solution of diethylamine in THF is added. The suspension is stirred at room temperature for 1 h. The precipitate is filtered off and the remaining solution is concentrated with a rotary evaporator to yield tetrabutylammonium-4-diethylaminobutylsulfonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642778B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-ecdb818b27aa4fe0be30d44cddbcb227 |
| Source note | uspto-grants-2014_02 |