Diethylamine → HCID 56973005, compound

HRID 239198Notes

Reaction equation

HRID 239198 reaction equation
[CH2:1]([N+:5]([CH2:14][CH2:15][CH2:16][CH3:17])([CH2:10][CH2:11][CH2:12][CH3:13])[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].Cl[CH2:19][CH2:20][CH2:21][CH2:22][S:23]([O-:26])(=[O:25])=[O:24].[CH2:27]([NH:29][CH2:30][CH3:31])[CH3:28]>C1COCC1>[CH2:14]([N+:5]([CH2:1][CH2:2][CH2:3][CH3:4])([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:10][CH2:11][CH2:12][CH3:13])[CH2:15][CH2:16][CH3:17].[CH2:27]([N:29]([CH2:30][CH3:31])[CH2:19][CH2:20][CH2:21][CH2:22][S:23]([O-:26])(=[O:25])=[O:24])[CH3:28]

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 86654806HCID 86654806, compound

Product 1

HCID 56973005HCID 56973005, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

To a solution of tetrabutylammonium-4-chlorobutylsulfonate in THF sodium carbonate is added. To the resulting suspension, a solution of diethylamine in THF is added. The suspension is stirred at room temperature for 1 h. The precipitate is filtered off and the remaining solution is concentrated with a rotary evaporator to yield tetrabutylammonium-4-diethylaminobutylsulfonate.

Workup

  1. filtrationThe precipitate is filtered off
  2. concentrationthe remaining solution is concentrated with a rotary evaporator

Sources & evidence

ORD record
ord-ecdb818b27aa4fe0be30d44cddbcb227
Source dataset
uspto-grants-2014_02
Patent number
US08642778B2

Reaction notes

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