Phenylhydrazine → HCID 21860261, compound

HRID 2392521Notes

Reaction equation

HRID 2392521 reaction equation
CS[C:3](=[C:9]([C:12]#[N:13])[C:10]#[N:11])[C:4]1[S:5][CH:6]=[CH:7][CH:8]=1.[C:14]1([NH:20][NH2:21])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[NH2:11][C:10]1[N:20]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:21]=[C:3]([C:4]2[S:5][CH:6]=[CH:7][CH:8]=2)[C:9]=1[C:12]#[N:13]

Participants

3

Reactant 2

HCID 7516PhenylhydrazineHCID 13150026HCID 13150026, compound

Product 1

HCID 21860261HCID 21860261, compound

Procedure

Using 2.06 g (10 mmol) of methylthio(thiophen-2-yl)methylenepropanedinitrile and 1.1 g (10 mmol) of phenylhydrazine, the entitled product having a melting point of 165° to 167° C. was obtained in the same manner as in Example 1-(1).

Sources & evidence

ORD record
ord-689a8d2a08cb4731a83dd0aeaa3a9064
Source dataset
uspto-grants-1998_09
Patent number
US05801008

Reaction notes

Loading…