Phenylhydrazine → HCID 21860262, compound

HRID 2392523Notes

Reaction equation

[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[CH:3]=[C:2]1[C:10](=[C:13]([C:16]#[N:17])[C:14]#[N:15])SC.[C:18]1([NH:24][NH2:25])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[NH2:15][C:14]1[N:24]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[N:25]=[C:10]([C:2]2[S:1][C:5]3[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=3[CH:3]=2)[C:13]=1[C:16]#[N:17]

Participants

Reactant 2

HCID 7516Phenylhydrazine

HCID 13150023HCID 13150023, compound

Product 1

HCID 21860262HCID 21860262, compound

Procedure

Using 2.56 g (10 mmol) of (benzothiophen-2-yl) (methylthio)methylenepropanedinitrile and 1.1 g (10 mmol) of phenylhydrazine, the entitled product having a melting point of 260° to 262° C. was obtained in the same manner as in Example 1-(1).

Sources & evidence

ORD record: ord-dd309c527666480bac68cb6029791f61
Source dataset: uspto-grants-1998_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05801008

Reaction notes

Loading…