HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Nitrophenyl)-1H-1,2,4-triazole → 4-(1,2,4-Triazol-1-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Nitrophenyl)-1H-1,2,4-triazole | HCID 11095398 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(1,2,4-Triazol-1-yl)aniline | HCID 735826 | 87% |
Reaction Steps
4-(1,2,4-Triazol-1-yl)nitrobenzene (0.5 g, 3 mmol) and Pd/C (500 mg) in ethanol (50 ml) were hydrogenated at rtp for 3 days. The suspension was filtered through celite, evaporated under reduced pressure to afford a white solid (418 mg, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801170 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-464669df42a34bb8ac4435d69214ab86 |
| Source note | uspto-grants-1998_09 |