HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Nitrophenyl)-2H-tetrazole → 4-(2H-1,2,3,4-tetrazol-2-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Nitrophenyl)-2H-tetrazole | HCID 533883 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(2H-1,2,3,4-tetrazol-2-yl)aniline | HCID 571639 | 114% |
Reaction Steps
4-(Tetrazol-2-yl)nitrobenzene (0.83 g, 4.3 mmol) and Pd/C (300 mg) in ethanol (50 ml) were hydrogenated at rtp for 3 days. The suspension was filtered through celite, evaporated under reduced pressure to afford a white solid (790 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801170 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-73dc5d7ccca44ef1825e112fff6079eb |
| Source note | uspto-grants-1998_09 |