HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Methyl-4-nitrophenyl)-1,2,4-triazole → 2-Methyl-4-[1,2,4]triazol-1-yl-phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Methyl-4-nitrophenyl)-1,2,4-triazole | HCID 14450248 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Methyl-4-[1,2,4]triazol-1-yl-phenylamine | HCID 14450262 | 100% |
Reaction Steps
2-Methyl-4-(1,2,4-Triazol-1-yl)nitrobenzene (1.0 g, 4.9 mmol) and Pd/C (200 mg) in ethanol (50 ml) were hydrogenated at rtp for 3 days. The suspension was filtered through celite, evaporated under reduced pressure to afford a white solid (850 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801170 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-3f9db7cc5dc84c3a98acce919db0185d |
| Source note | uspto-grants-1998_09 |