Potassium Bromide → HCID 18980387, compound

Participants

Reaction Steps

The title compound was prepared according to the general procedure described in Example 6 by substituting 8 mmol of 129 for 125. Yield: 91%; mp 238°-240° C. (from EtOH); IR (KBr) 3436, 3046, 2926, 2855, 1652, 1618, 1597, 1374, 1363 and 1263 cm-1 ; 1H NMR (in DMSO-d6) δ3.73 (s, 3H), 7.00 (m, 1H), 7.18 (m, 2H), 7.20 (s, 1H), 7.36 (m, 1H), 7.52 (s, 1H), 8.28 (s, 1H), 12.57 (br.s, 1H, N--H); HPLC: 100%; HRMS Calcd for C15H10N2O3Cl2 : 336.0068. Found: 336.0075.

Provenance & Evidence