Potassium Bromide → HCID 18980367, compound

Participants

Reaction Steps

The title compound was prepared according to the general procedure described in Example 6 by substituting 8 mmol of 131 for 125. Yield: 50%; mp 239°-241° C. (from EtOH); IR (KBr) 3459, 3050, 2958, 2796, 1651, 1618, 1375 and 1257 cm-1 ; 1H NMR (in DMSO-d6) δ3.69 (s, 3H), 7.00 (dd, 1H, JJ=7.4 Hz), 7.10 (d, 1H, J=7.4 Hz), 7.26 (d, 1H, J=7.4 Hz), 7.46 (dd, 1H, JJ=7.4 Hz), 7.54 (s, 1H), 8.26 (s, 1H), 12.58 (br.s, 1H, N--H); HPLC: 98%; HRMS Calcd for C15H10 N2O3Cl2 : 336.0068. Found: 336.0078.

Provenance & Evidence