Potassium Bromide → HCID 18980371, compound

Participants

Reaction Steps

The title compound was prepared according to the general procedure described in Example 6 by instituting 8 mmol of 133 for 125. Yield: 97%; mp 260°-262° C. (from EtOH); IR (KBr) 3454, 3044, 2923, 2801, 1653, 1617, 1380, 1364, 1311 and 1245 cm-1 ; 1H NMR (in DMSO-d6) δ2.31 (s, 3H), 7.23 (m, 1H,), 7.33 (m, 1H), 7.43 (m, 1H), 7.44 (s, 1H, 7.51 (s, 1H), 8.27 (s, 1H), 12.59 (br.s, 1H, N--H); HPLC: 97%; HRMS Calcd for C15H10N2O2Cl2 : 320.0119.

Provenance & Evidence