HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromoanisole → HCID 18980486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromoanisole | HCID 16971 | — |
| Reactant | HCID 18980511 | HCID 18980511 | — |
| Product | HCID 18980486 | HCID 18980486 | 37% |
Reaction Steps
Base (13) was reacted with 1-bromo-3-methoxy-benzene corresponding to the conditions described in Example 1. The base obtained was purified with 1:4 ether/diisopropyl ether via a silica gel column and was taken up in 1:1 2-butanone/ether. After adding trimethylchlorosilane/water, compound (10) was obtained in a yield of 37% theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801201 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-000dff36fe924baab08712cf5e4f3eb9 |
| Source note | uspto-grants-1998_09 |