反应详情

The base of compound (27) was reacted with 1-bromo-3-(2-methyl-allyloxy)-benzene corresponding to the conditions described in Example 1. The base obtained was purified with ether via a silica gel column and was taken up in 2-butanone. After adding trimethylchlorosilane/water, compound (31) was obtained in a yield of 51% theoretical. melting point: 193° C.-195° C.

1. customThe base obtained
2. customwas purified with ether via a silica gel column
3. additionAfter adding trimethylchlorosilane/water