HuagongsheHuagongshe Chemistry Print Report · For research reference only
192870-97-6 → HCID 18980462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 192870-97-6 | HCID 15816719 | — |
| Reactant | HCID 18980453 | HCID 18980453 | — |
| Product | HCID 18980462 | HCID 18980462 | 51% |
Reaction Steps
The base of compound (27) was reacted with 1-bromo-3-(2-methyl-allyloxy)-benzene corresponding to the conditions described in Example 1. The base obtained was purified with ether via a silica gel column and was taken up in 2-butanone. After adding trimethylchlorosilane/water, compound (31) was obtained in a yield of 51% theoretical. melting point: 193° C.-195° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801201 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-567e1ae6289e4e6fa33cf391c613d585 |
| Source note | uspto-grants-1998_09 |