HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18980432, compound → HCID 18980472, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18980432 | HCID 18980432 | — |
| Reactant | Ethyl ether methylene chloride | HCID 21881112 | — |
| Product | HCID 18980472 | HCID 18980472 | 56% |
Reaction Steps
Compound (43) was hydrogenated corresponding to the conditions described in Example 23, step 2. The product was then taken up in 1:1 dichloromethane/ether and tetramethylchlorosilane/water was added. After recrystallisation from 2-butanone/water, compound (39) was obtained in a yield of 56% theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801201 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-040c6757c52d42b9a50b30e8a1f2fdc8 |
| Source note | uspto-grants-1998_09 |