HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-phenylethane → HCID 53837619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-phenylethane | HCID 231496 | — |
| Reactant | 1,4-Dioxaspiro[4.5]decan-8-one | HCID 567415 | — |
| Product | HCID 53837619 | HCID 53837619 | 71% |
Reaction Steps
(2-chloroethyl)-benzene was reacted with 1,4-dioxa-spiro[4.5]decan-8-one corresponding to the conditions described in Example 24, step 1. The product was purified with 5:1 ether/n-hexane on a silica gel column. Compound (46) was obtained in a yield of 71% theoretical.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05801201 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-471e9eb3def34d97a98dce6d4f6eee7e |
| Source note | uspto-grants-1998_09 |