huagongshe.com
HRID2392759

反应详情

EQUATION

反应方程式

HRID 2392759 的结构方程式

REACTANTS

反应物

2
结构：Brc1cccc(OCc2ccccc2)c1
HCID2756638

3-Benzyloxybromobenzene

C13H11BrO

结构：CN(C)CC1CC(CCc2ccccc2)CCC1=O.Cl
HCID18980416

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CC1CC(CCc2ccccc2)CCC1(O)c1cccc(OCc2ccccc2)c1
HCID18980508

未命名化合物

收率 87%

PROCEDURE

实验过程

The base of compound (48) was reacted with 1-bromo-3-benzyloxy-benzene corresponding to the conditions described in Example 1. The base obtained was purified with 6:1 ether/methanol via a silica gel column. Compound (50) was obtained in a yield of 87% theoretical.

WORKUP

后处理

  1. customThe base obtained
  2. customwas purified with 6:1 ether/methanol via a silica gel column