HRID2392843

反应详情

EQUATION

反应方程式

HRID 2392843 的结构方程式

PROCEDURE

实验过程

100 ml of a 3.7% strength by weight sodium hydrogen carbonate solution (44.1 mmol NaHCO3) are added to 15.0 g (44.1 mmol) of (4-diphenylphosphinophenyl)methylphosphinic acid and the mixture stirred at room temperature until CO2 formation has ended. The aqueous solution is completely evaporated and dried under reduced pressure. 15.6 g (97% of theory) of sodium (4-diphenylphosphinophenyl)methylphosphinate are obtained. Solubility in water: 590 g/l

WORKUP

后处理

  1. customThe aqueous solution is completely evaporated
  2. customdried under reduced pressure