HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylbenzoyl chloride → N-(4-t-Butylbenzoyl)-4-(2-bromoethyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylbenzoyl chloride | HCID 74372 | — |
| Reactant | 4-(2-Bromoethyl)benzenesulfonamide | HCID 14485091 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | N-(4-t-Butylbenzoyl)-4-(2-bromoethyl)benzenesulfonamide | HCID 18977847 | — |
Reaction Steps
A mixture of 26.41 g (0.10 mol) of 4-(2-bromoethyl)benzenesulfonamide, 19.67 g (0.10 mol) of 4-t-butylbenzoyl chloride and 160 ml of xylene was heated at reflux for 20 hrs. The hot solution was cooled and the solid which crystallized was collected, recrystallized from isopropanol collected, washed with ligroine and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05804348 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-23c317b380a94066a46fe7c4f084d972 |
| Source note | uspto-grants-1998_09 |