huagongshe.com
HRID2392982

反应详情

EQUATION

反应方程式

HRID 2392982 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1ccc(C(=O)Cl)cc1
HCID74372

Benzoyl chloride, 4-(1,1-dimethylethyl)-

C11H13ClO

结构：NS(=O)(=O)c1ccc(CCBr)cc1
HCID14485091

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)c1ccc(C(=O)NS(=O)(=O)c2ccc(CCBr)cc2)cc1
HCID18977847

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1C
溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

A mixture of 26.41 g (0.10 mol) of 4-(2-bromoethyl)benzenesulfonamide, 19.67 g (0.10 mol) of 4-t-butylbenzoyl chloride and 160 ml of xylene was heated at reflux for 20 hrs. The hot solution was cooled and the solid which crystallized was collected, recrystallized from isopropanol collected, washed with ligroine and dried.

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureat reflux for 20 hrs
  3. temperatureThe hot solution was cooled
  4. customthe solid which crystallized
  5. customwas collected
  6. customrecrystallized from isopropanol
  7. customcollected
  8. washwashed with ligroine
  9. customdried