Allylamine → HCID 14093037, compound

To a cooled solution of 125 mL aqueous allylamine (60%), 3-chloropropionic acid (20 g) was added portionwise while stirring over 5 minutes. The mixture was stirred at ambient temperature for 72 hours. The mixture was then evaporated to a viscous oily residue (40 g). The product consisted of a 1:1 mixture of 3-allylaminopropionic acid and allylamine hydrochloride. This product mixture was used without further purification for the preparation of the title compound in step 2.

1. stirringThe mixture was stirred at ambient temperature for 72 hours
2. customThe mixture was then evaporated to a viscous oily residue (40 g)
3. additionThe product consisted of a 1:1 mixture of 3-allylaminopropionic acid and allylamine hydrochloride
4. customThis product mixture was used without further purification for the preparation of the title compound in step 2

ORD record

ord-2ecb17d935214b2d958d921f99cb3ffa

Source dataset

uspto-grants-1998_09

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US05807864