HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9861000, compound → HCID 9860999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9861000 | HCID 9861000 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 9860999 | HCID 9860999 | — |
Reaction Steps
1-[1-(9H-Fluoren-2-yl)ethyl]-1H-imidazole (8.88 g) was dissolved in ethyl acetate, and 15 ml of 4N hydrogen chloride-ethyl acetate was added to this solution under ice-cooling. The thus precipitated crystals were collected by filtration and washed with ethyl acetate to obtain 9.95 g of 1-[1-(9H-fluoren-2-yl)ethyl]-1H-imidazole hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05807880 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-7120ebce76b4411dbe07352080f89e2a |
| Source note | uspto-grants-1998_09 |