HCID 9861000, compound → HCID 9860999, compound

HRID 2393502Notes

Reaction equation

HRID 2393502 reaction equation
[CH:1]1[C:13]2[CH2:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][C:2]=1[CH:14]([N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)[CH3:15].C(OCC)(=O)C.[ClH:27]>C(OCC)(=O)C>[ClH:27].[CH:1]1[C:13]2[CH2:12][C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][C:2]=1[CH:14]([N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)[CH3:15]

Participants

4

Reactant 2

HCID 9861000HCID 9861000, compoundHCID 21866389Hydrogen chloride-ethyl acetate

Product 1

HCID 9860999HCID 9860999, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

1-[1-(9H-Fluoren-2-yl)ethyl]-1H-imidazole (8.88 g) was dissolved in ethyl acetate, and 15 ml of 4N hydrogen chloride-ethyl acetate was added to this solution under ice-cooling. The thus precipitated crystals were collected by filtration and washed with ethyl acetate to obtain 9.95 g of 1-[1-(9H-fluoren-2-yl)ethyl]-1H-imidazole hydrochloride.

Workup

  1. temperaturecooling
  2. filtrationThe thus precipitated crystals were collected by filtration
  3. washwashed with ethyl acetate

Sources & evidence

ORD record
ord-7120ebce76b4411dbe07352080f89e2a
Source dataset
uspto-grants-1998_09
Patent number
US05807880

Reaction notes

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