HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 15407842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 10911969 | HCID 10911969 | — |
| Product | HCID 15407842 | HCID 15407842 | — |
Reaction Steps
Under an inert atmosphere, [5H]-7,12-dioxa-5-azabenz[a]anthracen-6-one is brought to reflux of phosphorus oxychloride for 6 hours. The solvent (phosphorus oxychloride) is then evaporated off under vacuum and the crude mixture is chromatographed by flash chromatography on silica gel (eluent: petroleum ether/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05807882 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-4df38f854e2f4ce980fb69780e1a3713 |
| Source note | uspto-grants-1998_09 |