HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl propiolate → HCID 18976127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl propiolate | HCID 13536 | — |
| Reactant | HCID 18976112 | HCID 18976112 | — |
| Product | HCID 18976127 | HCID 18976127 | — |
Reaction Steps
In a sealed tube, 500 mg of 2-(1-cyclohexenyl)-1,4-benzodioxin and 1.4 ml of methyl propiolate are stirred for 22 hours 30 minutes at 70° C. The regioisomers are separated by chromatography on silica gel (eluent: petroleum ether/ethyl acetate, 98:2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05807882 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-a1405b7313c142409d8c6ab922ed6cca |
| Source note | uspto-grants-1998_09 |