HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Disulfide → HCID 70104303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Disulfide | HCID 12232 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 70105092 | HCID 70105092 | — |
| Reactant | HCID 178461630 | HCID 178461630 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70104303 | HCID 70104303 | — |
Reaction Steps
2.4 g of the expected product from Stage B is dissolved in 25 cm3 of anhydrous THF. 3 ml of a 3M solution of EtMgBr in ether is added. After 1 hour at ambient temperature, 1.08 cm3 of dimethyl disulphide is added and the reaction medium is left for 1 hour at ambient temperature followed by hydrolysis with saturated NH4Cl, extraction with AcOEt, drying and evaporating to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05807878 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-c7a985f3e35e473483812ec28ea426dd |
| Source note | uspto-grants-1998_09 |