HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136381101, compound → HCID 178491207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136381101 | HCID 136381101 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178491207 | HCID 178491207 | 58% |
Reaction Steps
Prepared analogously to Example 1c) from N5 -[amino(nitroimino)methyl)-N-[(3,4-dimethoxyphenyl)-methyl]-N2 -(diphenylacetyl)-ornithinamide by catalytic hydrogenation in the presence of palladium black and 80% aqueous acetic acid in a yield of 58% of theory. Colourless amorphous substance Rf 0.62.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05807875 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-2166054e1f694e678dbe7e28f700f544 |
| Source note | uspto-grants-1998_09 |