HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 10858299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 10781998 | HCID 10781998 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10858299 | HCID 10858299 | — |
Reaction Steps
The title compound of Example 2B (1502 g, 4.18 mol) was dissolved in MeOH (2650 mL). While maintaining a temperature of 30° or below for the ensuing mixture, a cold solution of KOH (329 g, 5.85 mol) in H2O (1335 mL) was added dropwise over 20 min. The mixture was stirred vigorously for 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05808085 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-b4eeca4f23b44f1a9ee2fedf1a691f18 |
| Source note | uspto-grants-1998_09 |