Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 86749481 | HCID 86749481 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 86749480 | HCID 86749480 | — |
Reaction Steps
Next, 359 mg (1 mmol) of the methyl 2,3,4-tri-O-acetyl glucopyranuronosyl azide was added to 50 ml of tetrahyrofuran containing 50 mg of 10% Pd on carbon. The solution was cooled to -15° C. and was shaken under 40 psl of hydrogen for 1 hour, filtered and concentrated to dryness to produce methyl 2,3,4,-tri-O-acetylglucopyranuronosyl amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05808111 |
|---|
| Source dataset | uspto-grants-1998_09 |
|---|
| ORD ID | ord-cae1f3287a8c4e04be7a94492debe84a |
|---|
| Source note | uspto-grants-1998_09 |
|---|
