HRID2394079

反应详情

EQUATION

反应方程式

HRID 2394079 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of the compounds according to Example Ia-3 and Ia-4 (cis-trans mixture) (300 mg), trifluoroacetic acid (10 ml) and water (10 ml) is stirred at room temperature for 24 hours and concentrated. The solid residue is washed with hot cyclohexane.

WORKUP

后处理

  1. additionA mixture of the compounds
  2. concentrationconcentrated
  3. washThe solid residue is washed with hot cyclohexane