HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 15152395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 5-chloro-6-methylpyrazine-2-carboxylate | HCID 12619146 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15152395 | HCID 15152395 | 39% |
Reaction Steps
A mixture of methyl 5-chloro-6-methyl-2-pyrazine carboxylate (0.16 g, 0.86 mmol), K2CO3 (0.31 g, 2.18 mmol) and H2O was stirred for 2 h at room temperature. The reaction was filtered and acidified (20% HCl), and the resulting solid collected to provide the title compound (0.057 g, 39% yield); m.p. 116°-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811428 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-e92157a3c8034bb987e920aa60e19fa5 |
| Source note | uspto-grants-1998_09 |