HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136351329, compound → HCID 178469225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136351329 | HCID 136351329 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | HCID 178469225 | HCID 178469225 | — |
Reaction Steps
102.7 g (0.35 mol) of ethyl 4,5,5-trichloro-3-hydroxy-2-(1-imino-ethyl)penta-2,4-dienoate are heated at 180° C. in 1,2-dichlorobenzene for three hours. The volatile components are removed under a high vacuum up to 100° C. The residue is purified with dichloromethane on silica gel.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811433 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-4fc64a4759fd49dbb8342f29b0d0376b |
| Source note | uspto-grants-1998_09 |