HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole-4-carboxaldehyde → HCID 18973527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole-4-carboxaldehyde | HCID 333703 | — |
| Reactant | 1-(Bromomethyl)-2,3-difluoro-benzene | HCID 517984 | — |
| Product | HCID 18973527 | HCID 18973527 | 77.6% |
Reaction Steps
The same procedures used in Example 1 were repeated except for using 580 mg of indole-4-carbaldehyde and 911 mg of 2,3-difluorobenzyl bromide in place of the benzyl bromide used in Example 1 to give 841 mg of 1-(2,3-difluorobenzyl)indole-4-carbaldehyde as pale brown crystals. The yield thereof was found to be 76%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811439 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-69f02546f12a4982a8910be803175d1d |
| Source note | uspto-grants-1998_09 |