HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole-4-carboxaldehyde → 1-(2-Thienylmethyl)indole-4-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole-4-carboxaldehyde | HCID 333703 | — |
| Reactant | 2-Thienylmethyl methanesulfonate | HCID 18973430 | — |
| Product | 1-(2-Thienylmethyl)indole-4-carbaldehyde | HCID 18973351 | — |
Reaction Steps
The same procedures used in Example 1 were repeated except for using 725 mg of indole-4-carbaldehyde and 2-thienylmethyl methanesulfonate instead of the benzyl bromide used in Example 1 to give 392 mg of 1-(2-thienylmethyl)indole-4-carbaldehyde as pale yellow crystals. The yield thereof was found to be 33%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811439 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-b94a6aca0ff0439087d60dd97479227e |
| Source note | uspto-grants-1998_09 |