HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydro-1,4-benzodioxin-2-ylmethyl methanesulfonate → HCID 86753136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydro-1,4-benzodioxin-2-ylmethyl methanesulfonate | HCID 263445 | — |
| Reactant | Indole-4-carboxaldehyde | HCID 333703 | — |
| Product | HCID 86753136 | HCID 86753136 | — |
Reaction Steps
The same procedures used in Example 1 were repeated except for using 870 mg of indole-4-carbaldehyde and 2-benzodioxanylmethyl methanesulfonate instead of the benzyl bromide used in Example 1 to give 699 mg of 1-(2-benzodioxanylmethyl)indole-4-carbaldehyde as a pale yellow oily substance. The yield thereof was found to be 40%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811439 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-b78744f8511748ce8977d97a4e3fa8dc |
| Source note | uspto-grants-1998_09 |