Hydrogen iodide → HCID 136377642, compound

HRID 2394808Notes

Reaction equation

HRID 2394808 reaction equation
C[O:2][C:3]1[CH:12]=[C:11]2[C:6]([C:7]([C:19]([OH:21])=[O:20])=[CH:8][C:9]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[N:10]2)=[CH:5][CH:4]=1.[IH:22]>>[IH:22].[OH:2][C:3]1[CH:12]=[C:11]2[C:6]([C:7]([C:19]([OH:21])=[O:20])=[CH:8][C:9]([C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)=[N:10]2)=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 24841Hydrogen iodideHCID 10802615HCID 10802615, compound

Product 1

HCID 136377642HCID 136377642, compound

Procedure

1.5 g (5.4 mmol) of 7-methoxy-2-phenylquinoline-4-carboxylic acid were added portionwise to 50 ml of 57% aqueous HI. The reaction mixture was refluxed and vigourously stirred for 5 hours; then it was evaporated in-vacuo to dryness to yield 2.1 g of the title compound.

Workup

  1. temperatureThe reaction mixture was refluxed
  2. customthen it was evaporated in-vacuo to dryness

Sources & evidence

ORD record
ord-5c1ff1bad9664ad88531a367fbd512ad
Source dataset
uspto-grants-1998_09
Patent number
US05811553

Reaction notes

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