HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-Methyl-3,4,6-trifluorobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methyl-3,4,6-trifluorobenzoic acid | HCID 10130305 | — |
| Product | 2-Methyl-3,4,6-trifluorobenzoyl chloride | HCID 15007607 | — |
Reaction Steps
To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thionyl chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811576 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-4c1ec2bcaa5b475f9759e36bc5507d2d |
| Source note | uspto-grants-1998_09 |