HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 4-[3-(2-Benzyloxyphenyl)propyl]benzene isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Reactant | 4-(3-(2-Benzyloxyphenyl)propyl]benzoic acid | HCID 18973764 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 4-[3-(2-Benzyloxyphenyl)propyl]benzene isocyanate | HCID 18973742 | — |
Reaction Steps
The solution of 4-[3-(2-benzyloxyphenyl)propyl]benzene isocyanate in dioxane was prepared by heating a mixture of 4-[3-(2-benzyloxyphenyl)propyl]benzoic acid (2.0 g), Et3N (1.61 ml) and DPPA (1.31 ml) in dioxane (20 ml) for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05811459 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-b83d6244966c4f20a0d16ffeccfa4409 |
| Source note | uspto-grants-1998_09 |