HRID2395044

反应详情

EQUATION

反应方程式

HRID 2395044 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The solution of 4-[3-(2-benzyloxyphenyl)propyl]benzene isocyanate in dioxane was prepared by heating a mixture of 4-[3-(2-benzyloxyphenyl)propyl]benzoic acid (2.0 g), Et3N (1.61 ml) and DPPA (1.31 ml) in dioxane (20 ml) for 3 hours.

WORKUP

后处理

  1. temperatureby heating